Use of experimental design in the optimization of stir bar sorptive extraction for the determination of polybrominated diphenyl ethers in environmental matrices.

@article{Serdio2007UseOE,
  title={Use of experimental design in the optimization of stir bar sorptive extraction for the determination of polybrominated diphenyl ethers in environmental matrices.},
  author={P Ser{\^o}dio and M. Salom{\'e} Cabral and Jos{\'e} Manuel Flor{\^e}ncio Nogueira},
  journal={Journal of chromatography. A},
  year={2007},
  volume={1141 2},
  pages={
          259-70
        }
}
Stir bar sorptive extraction and liquid desorption (LD) followed by large volume injection and capillary gas chromatography coupled to mass spectrometry (SBSE-LD-LVI-GC-MS), had been applied for the determination of ultra-traces of eleven polybrominated diphenylethers (PBDEs), from tetra to nona congeners (BDE-47, BDE-100, BDE-99, BDE-85, BDE-154, BDE-153, BDE-183, BDE-197, BDE-196, BDE-207 and BDE-206), in environmental matrices. Instrumental calibration under the selected-ion monitoring (SIM… CONTINUE READING

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