Two-dimensional NMR correlation experiments in the gas phase.


The application of common two-dimensional NMR correlation experiments to gaseous analytes for structural elucidation is reported. Standard sequences such as COSY, HSQC, and HMBC are readily applied to volatile hydrocarbons and fluorocarbons. In experiments using (19)F or (13)C as the observed nucleus, it is possible to take advantage of efficient spin… (More)
DOI: 10.1016/j.jmr.2011.02.005


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