Transverse-relaxation-optimized (TROSY) gradient-enhanced triple-resonance NMR spectroscopy.

  title={Transverse-relaxation-optimized (TROSY) gradient-enhanced triple-resonance NMR spectroscopy.},
  author={J Patrick Loria and Mark Rance and Arthur G. Palmer},
  journal={Journal of magnetic resonance},
  volume={141 1},
Two modifications to sensitivity-enhanced gradient-selected TROSY-based triple-resonance NMR experiments are proposed that reduce the overall duration of the pulse sequences and minimize radiation damping effects on water-flipback solvent suppression. The modifications are illustrated for the HNCO-TROSY experiment, but are applicable to all triple-resonance experiments that detect proton magnetization after a reverse polarization transfer step from a (15)N spin. The methods are applied to yeast… CONTINUE READING

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