The solubility and site preference of Fe3+ in Li7−3xFexLa3Zr2O12 garnets

  title={The solubility and site preference of Fe3+ in Li7−3xFexLa3Zr2O12 garnets},
  author={D Rettenwander and C. A. Geiger and Martina Tribus and Peter Tropper and Reinhard Wagner and Gerold Tippelt and Werner Lottermoser and Georg Amthauer},
  booktitle={Journal of solid state chemistry},
A series of Fe3+-bearing Li7La3Zr2O12 (LLZO) garnets was synthesized using solid-state synthesis methods. The synthetic products were characterized compositionally using electron microprobe analysis and inductively coupled plasma optical emission spectroscopy (ICP-OES) and structurally using X-ray powder diffraction and 57Fe Mössbauer spectroscopy. A maximum of about 0.25 Fe3+ pfu could be incorporated in Li7-3x Fe x La3Zr2O12 garnet solid solutions. At Fe3+ concentrations lower than about 0.16… CONTINUE READING
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