The mixed diol-dithiol 2,2-bis(sulfanylmethyl)propane-1,3-diol: characterization of key intermediates on a new synthetic pathway.

Abstract

A new synthetic route to 2,2-bis(sulfanylmethyl)propane-1,3-diol, (II), is described starting from the commercially available 2,2-bis(hydroxymethyl)propane-1,3-diol. The structures of two intermediates on this route are described. 5,5-Dimethenyl-2,2-dimethyl-1,3-dioxane bis(thiocyanate) (systematic name: {[5-(cyanosulfanyl)-2,2-dimethyl-1,3-dioxan-5-yl… (More)
DOI: 10.1107/S0108270110049371

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@article{Simmons2011TheMD, title={The mixed diol-dithiol 2,2-bis(sulfanylmethyl)propane-1,3-diol: characterization of key intermediates on a new synthetic pathway.}, author={Trevor R. Simmons and Christopher J. F. Pickett and Joseph A Wright}, journal={Acta crystallographica. Section C, Crystal structure communications}, year={2011}, volume={67 Pt 1}, pages={o1-5} }