The crystal structure of N-benzoyl-N-phenylhydroxylaminocarbonyltriphenylphosphinerhodium(I)

  title={The crystal structure of N-benzoyl-N-phenylhydroxylaminocarbonyltriphenylphosphinerhodium(I)},
  author={Johann G. Leipoldt and Elizabeth C. Grobler},
N-Benzoyl-N-phenylhydroxylaminocarbonyltriphenylphosphinerhodium(I), [Rh(BPHA)(CO)(PPh3)], was prepared by the reaction between [Rh(BPHA)(CO)2] and triphenylphosphine and recrystallized from acetone. The crystal structure of the compound was determined from 4572 unique observed reflections obtained with a computer automated diffractometer. The unit cell is triclinic with a = 14.723 A, b = 9.567 A, c = 10.328 A, α = 107.8°, β = 97.2°, γ = 82.9°, Z = 2 and space group P. The final R-value was 0… CONTINUE READING