Synthesis of spin-labelled 2-(16'-(N-oxyl-4'',4''-dimethyloxazolidine)stearoyl)-phosphatidylcholine.

Abstract

Chemical synthesis of spin-labelled lecithin 2-(16'-(N-oxyl-4'',4''-dimethyloxazolidine)stearoyl)-phosphatidylcholine was achieved by reaction of equimolar amounts of purified egg yolk lyso-lecithin with commercially available 16-(N-oxyl-4',4'-dimethyloxazolidine)stearic acid activated with N,N-carbonyldiimidazole. After purification by silicic acid column… (More)

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