Corpus ID: 97297654

Synthesis of 2-amino-4-(2 1 -nitro)phenyl-6(2 11 , 2 11 - dimethyl, 7 11 -hydroxy chroman) pyrimidine and study of their antimicrobial activity

@inproceedings{Murthy2009SynthesisO2,
  title={Synthesis of 2-amino-4-(2 1 -nitro)phenyl-6(2 11 , 2 11 - dimethyl, 7 11 -hydroxy chroman) pyrimidine and study of their antimicrobial activity},
  author={Y. Murthy and K. S. Varma and V. Satyanarayana},
  year={2009}
}
Resorcinol (1) was acylated using acetic acid in the presence of fused ZnCl 2 at 140-150 0 C for 15 min with stirring. The reaction mixture is left for 1hr and then 100ml of 1:1 HCl was added to break the zinc chloride complex and within 5 minutes precipitation commenced. The precipitate was washed with very dilute HCl and water. A red precipitate was obtained; which was crystallized from 20% HCl to give resacetophenone (II) needles and characterized by comparing its spectral data (IR, NMR… Expand

References

Biosynthesis of macromolecules
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