Corpus ID: 44157046

Synthesis and ESR and ENDOR Investigation of Phenalenyl Radical , a Useful ENDOR Reference Compound

@inproceedings{Ulbrich2012SynthesisAE,
  title={Synthesis and ESR and ENDOR Investigation of Phenalenyl Radical , a Useful ENDOR Reference Compound},
  author={A. Ulbrich and H. J. Sipe},
  year={2012}
}
  • A. Ulbrich, H. J. Sipe
  • Published 2012
  • Efforts to establish electron nuclear double resonance spectroscopy (ENDOR) are underway at Hampden-Sydney College. To this end, phenalenyl radical (PNT), a useful reference ENDOR compound, was successfully synthesized and ESR samples of the compound were prepared. The compound was prepared via a two step procedure from perinaphthenone. The perinapththenone was reacted with p-toluenesulfonylhydrazide and then the intermediate product was reduced to the radical by sodium borohydride and work-up… CONTINUE READING

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