Corpus ID: 101879991

Synthesis and Crystal Structure of 4-Azido-2,2,6,6-Tetramethylpiperidine-1-oxyl Free Radical

@article{Zhou2006SynthesisAC,
  title={Synthesis and Crystal Structure of 4-Azido-2,2,6,6-Tetramethylpiperidine-1-oxyl Free Radical},
  author={Zhou and Bao-Han and Chen and Yun-feng and Yin and Guo-dong and Wu and An-Xin},
  journal={Chinese Journal of Structural Chemistry},
  year={2006},
  volume={25},
  pages={127-130}
}
  • Zhou, Bao-Han, +5 authors An-Xin
  • Published 2006
  • Chemistry
  • Chinese Journal of Structural Chemistry
The title compound 4-azido-2,2,6,6-tetramethylpiperidine-1-oxyl (C9H17N4O, Mr = 197.27) has been synthesized and its structure was determined by single-crystal X-ray diffraction. The crystal belongs to triclinic, space group P1 with a = 5.8464(12), b = 8.2476(17), c = 11.954(2) ?, a = 101.973(4), a = 97.186(3), ? = 100.232(3)o, V = 546.98(19) ?3, Z = 2, Dc = 1.198 g/cm3, i(MoKa) = 0.082 mm–1, F(000) = 214, R = 0.0495 and wR = 0.1355 for 1677 observed reflections with I 2σ(I). X-ray analysis… Expand