• Corpus ID: 212535028

Synthesis, characterization and catalytic application of MgO supported metal catalysts in synthesis of dihydropyrimidinone

@inproceedings{Anvekar2017SynthesisCA,
  title={Synthesis, characterization and catalytic application of MgO supported metal catalysts in synthesis of dihydropyrimidinone},
  author={Tushar Shamba Anvekar and Kanika K. Korgaonkar},
  year={2017}
}

• T. Anvekar, Kanika K. Korgaonkar
• Published 2017
• Chemistry

In the present investigation, syntheses of different metal supported MgO prepared by two different ways viz.; (a) Sol Ni/MgO, Co/MgO and Ru/MgO catalysts and (b) Impregnation method for synthesis of 20% Ni/ catalysts samples were characterized using instrumental techniques such as XRD, SEM, FT reveals that samples possess particle size of 8.420 nm and 17.439 nm at 2 SEM micrographs shows that the particles possesses irregular shape and are generally random, non with particle size approximately <100 nm . All the catalysts supported on MgO are found as amorphous in nature. The IR spectra gives fundamental band for Mg-O at 1384 cm support. The BET analysis depicts the surface area of 91.1 m follows the micro porous structure of the prepared samples. The catalytic activity of the Ni/Mgo and Co/MgO has been investigated for the Biginelli reaction for synthesis of dihydropyrimidinone. The supported catalysts were found to be active for synthesis of dihydropyrimidinone. Co/MgO su support.