Synthesis, Spectroscopic Studies and Crystal Structure of N,N′-bis((thiophene-2-carboxamido)propyl)piperazine

  title={Synthesis, Spectroscopic Studies and Crystal Structure of N,N′-bis((thiophene-2-carboxamido)propyl)piperazine},
  author={Ayla Balaban and Naki Çolak and H{\"u}seyin {\"U}nver and Birg{\"u}l Erk and Tahsin Nuri Durlu and D. Mehmet Zengin},
  journal={Journal of Chemical Crystallography},
AbstractA new multidentate ligand N,N′-bis((thiophene-2-carboxamide)propyl)piperazine has been synthesized from the reaction of thiophene-2-carbonylchloride and 1,4-bis(3-aminopropyl)piperazine. The title compound has been characterized by elemental analysis, FT-IR, 1H-NMR and 13C-NMR spectroscopic techniques. The crystal structure of the title compound (C20H30N4O2S2Cl2) has also been determined by X-ray analysis. The title compound crystallize in the monoclinic space group P21/c with a = 9.768… CONTINUE READING