Sulfonyl Fluoride Synthesis through Electrochemical Oxidative Coupling of Thiols and Potassium Fluoride

@inproceedings{Laudadio2019SulfonylFS,
  title={Sulfonyl
Fluoride Synthesis through Electrochemical
Oxidative Coupling of Thiols and Potassium Fluoride},
  author={Gabriele Laudadio and Aloisio de Andrade Bartolomeu and Lucas M H M Verwijlen and Yiran Cao and Kleber Thiago de Oliveira and Timothy No{\"e}l},
  booktitle={Journal of the American Chemical Society},
  year={2019}
}
Sulfonyl fluorides are valuable synthetic motifs for a variety of applications, amongst which SuFEx-based click chemistry is currently the most prominent. Consequently, the development of novel and efficient synthetic methods to access these functional groups is of great interest. Herein, we report a mild and environmentally benign electrochemical approach to prepare sulfonyl fluorides using thiols or disulfides, as widely available starting materials, in combination with KF, as an inexpensive… CONTINUE READING

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