Solution-state 2D NMR of ball-milled plant cell wall gels in DMSO-d(6)/pyridine-d(5).

@article{Kim2010Solutionstate2N,
  title={Solution-state 2D NMR of ball-milled plant cell wall gels in DMSO-d(6)/pyridine-d(5).},
  author={Hoon Kim and John Ralph},
  journal={Organic & biomolecular chemistry},
  year={2010},
  volume={8 3},
  pages={576-91}
}
NMR fingerprinting of the components of finely divided plant cell walls swelled in DMSO has been recently described. Cell wall gels, produced directly in the NMR tube with perdeutero-dimethylsulfoxide, allowed the acquisition of well resolved/dispersed 2D (13)C-(1)H correlated solution-state NMR spectra of the entire array of wall polymers, without the need for component fractionation. That is, without actual solubilization, and without apparent structural modification beyond that inflicted by… CONTINUE READING
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