Solid-state NMR study of trehalose/1,2-dipalmitoyl-sn-phosphatidylcholine interactions.

@article{Lee1986SolidstateNS,
  title={Solid-state NMR study of trehalose/1,2-dipalmitoyl-sn-phosphatidylcholine interactions.},
  author={Choon Woo Lee and J S Waugh and Robert G Griffin},
  journal={Biochemistry},
  year={1986},
  volume={25 13},
  pages={3737-42}
}
31P and 2H solid-state NMR studies of dry trehalose (TRE) and 1,2-dipalmitoyl-sn-phosphatidylcholine (DPPC) mixtures are reported. 31P spectra are consistent with a rigid head group above and below the calorimetric phase transition for both dry DPPC and a dry 2:1 TRE/DPPC mixture. In addition, 2H spectra of DPPC labeled at the 7-position of the sn-2 chain (2[7,7-2H2]DPPC) show exchange-narrowed line shapes with a width of 120 kHz over the temperature range 25-75 degrees C. These line shapes can… CONTINUE READING

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