Solid-phase extraction and cleanup procedures for determination of acrylamide in fried potato products by liquid chromatography/mass spectrometry.

@article{Young2004SolidphaseEA,
  title={Solid-phase extraction and cleanup procedures for determination of acrylamide in fried potato products by liquid chromatography/mass spectrometry.},
  author={Michael E. S. Young and Kevin M. Jenkins and Claude Mallet},
  journal={Journal of AOAC International},
  year={2004},
  volume={87 4},
  pages={
          961-4
        }
}
In response to recent discoveries of acrylamide in heated foods, a solid-phase extraction and cleanup protocol was developed for the determination of acrylamide in fried or baked potato samples by liquid chromatography/mass spectrometry (LC/MS). The analyte was extracted from the matrix by using 2M NaCl, and an aliquot of the initial extract was loaded onto a reversed-phase cartridge. After the analyte was eluted from the cartridge, the eluate was cleaned up on a mixed-mode cation-exchange… CONTINUE READING

Similar Papers