Simultaneous determination of six quinolones in pig muscle by liquid chromatography-atmospheric pressure chemical ionisation mass spectrometry.

@article{Delepine1998SimultaneousDO,
  title={Simultaneous determination of six quinolones in pig muscle by liquid chromatography-atmospheric pressure chemical ionisation mass spectrometry.},
  author={Bernard Delepine and Dominique Hurtaud-Pessel and Pascal Sand{\'e}rs},
  journal={The Analyst},
  year={1998},
  volume={123 12},
  pages={2743-7}
}
An LC-MS method is described for the confirmation of six quinolones (enrofloxacine, ciprofloxacine, marbofloxacine, danofloxacine, sarafloxacine and difloxacine) in pig muscle. The quinolones were extracted from muscle (2 g) with phosphate buffer (pH 7.4). After centrifugation, the extract was purified on a C18 solid-phase extraction cartridge. Samples were analysed by LC with gradient elution on a C18 column and detected by MS via an atmospheric pressure chemical ionisation interface. For each… CONTINUE READING

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