Simultaneous determination of eight underivatised biogenic amines in fish by solid phase extraction and liquid chromatography-tandem mass spectrometry.

@article{Sagratini2012SimultaneousDO,
  title={Simultaneous determination of eight underivatised biogenic amines in fish by solid phase extraction and liquid chromatography-tandem mass spectrometry.},
  author={Gianni Sagratini and M{\'o}nica Fern{\'a}ndez-Franz{\'o}n and Franco De Berardinis and Guillermina Font and Sauro Vittori and Jordi Ma{\~n}es},
  journal={Food chemistry},
  year={2012},
  volume={132 1},
  pages={537-43}
}
Biogenic amines on fish tissue are formed as a result of bacterial contamination and spoilage during storage. A new method based on liquid chromatography (LC) and tandem mass spectrometry (MS/MS) using a triple quadrupole (QqQ) analyser was developed for the analysis of eight biogenic amines (cadaverine, histamine, phenylethylamine, putrescine, spermine, spermidine, tyramine and tryptamine) in fish tissues. Sample preparation was performed by extraction with trichloroacetic acid 5% and solid… CONTINUE READING
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