Simultaneous determination of 38 veterinary antibiotic residues in raw milk by UPLC-MS/MS.

  title={Simultaneous determination of 38 veterinary antibiotic residues in raw milk by UPLC-MS/MS.},
  author={Rongwei Han and N Zheng and Zhongqing Yu and Jianpeng Wang and Xiao Xu and Xiaoxia Qu and Songli Li and Yangdong Zhang and Jiaqi Wang},
  journal={Food chemistry},
A selective and rapid method has been developed to determine, simultaneously, 38 veterinary antibiotic residues in raw milk by ultra-high-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). One milliliter of raw milk was diluted with 0.5 mL water and 3 mL acetonitrile, then purified using an Oasis HLB cartridge. The eluates were evaporated by nitrogen drying and then reconstituted to 4 mL with water/acetonitrile (8:1) before being injected into the UPLC-MS/MS system. The… CONTINUE READING
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