Simultaneous determination of 13 aminoglycoside residues in foods of animal origin by liquid chromatography-electrospray ionization tandem mass spectrometry with two consecutive solid-phase extraction steps.

@article{Zhu2008SimultaneousDO,
  title={Simultaneous determination of 13 aminoglycoside residues in foods of animal origin by liquid chromatography-electrospray ionization tandem mass spectrometry with two consecutive solid-phase extraction steps.},
  author={Wei-xia Zhu and Ji-zhou Yang and Wei Wei and Ya-feng Liu and Shusheng Zhang},
  journal={Journal of chromatography. A},
  year={2008},
  volume={1207 1-2},
  pages={29-37}
}
A confirmatory and quantitative method based on liquid chromatography-electrospray ionization tandem mass spectrometry (LC-ESI-MS/MS) has been developed for simultaneous determination of 13 aminoglycoside antibiotics in various samples. The aminoglycoside analytes were released and extracted from different matrices with 5% trichloroacetic acid. The influence of pH values on the solid-phase exaction (SPE) procedure has been studied. Due to different pK(a) values of the compounds, seven… CONTINUE READING

Citations

Publications citing this paper.
Showing 1-9 of 9 extracted citations

Validation of two ELISA kits for the screening of tylosin and streptomycin in honey according to the European decision 2002/657/EC.

Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment • 2013
View 2 Excerpts

References

Publications referenced by this paper.
Showing 1-2 of 2 references

J

Y. Cai, J. Cheng, S. Mou, Y. Lu
Chromatogr. A 1085 • 2005

Antimicrob

A. P. Provoost, W. V. Schalkwijk, O. Adejuyigbe, W. V. Leeuwen, J. T. Wagenvoort
Agents Chemother. 25 (1984) 497. [8] M. Preu, D. Guyot, M. Petz, J. Chromatogr. A 818 • 1998
View 3 Excerpts

Similar Papers

Loading similar papers…