• Corpus ID: 101846205

Simultaneous Determination of Zoalene ant Its Metabolite in Chicken Tissues by Ultra Performance Liquid Chromatography

@article{Yin2011SimultaneousDO,
  title={Simultaneous Determination of Zoalene ant Its Metabolite in Chicken Tissues by Ultra Performance Liquid Chromatography},
  author={Wu Yin},
  journal={Chinese Journal of Analytical Chemistry},
  year={2011}
}
  • W. Yin
  • Published 2011
  • Chemistry
  • Chinese Journal of Analytical Chemistry
A method was developed for the simultaneous determination of zoalene and its metabolite(3-Amino-5-nitro-o-toluamide,ANOT) in chicken tissues by ultra performance liquid chromatog-raphy(UPLC).Samples were extracted twice with acidic phosphate buffer solution and then the extracts were adjusted to pH 7.0 and purified through HLB cartridge after centrifugation.The residues were eluted from cartridge with 0.1% formic acid solution/acetonitrile(80 ∶ 20,V/V).The samples were analyzed by UPLC with… 
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Development of an ASE-GC-MS/MS method for detecting dinitolmide and its metabolite 3-ANOT in eggs.

TLDR
An accelerated solvent extraction coupled with gas chromatography-tandem mass spectrometry (ASE-GC-MS/MS) method for detecting dinitolmide residue and its metabolite (3-amino-2-methyl-5-nitrobenzamide, 3-ANOT) in eggs was developed and optimized and successfully applied to the quantitative determination.