Simple one-pot regioselective 6-O-phosphorylation of carbohydrates and trehalose desymmetrization.


Biologically essential carbohydrate 6-phosphates, especially trehalose 6-phosphate, can be synthesized easily in excellent overall yields in 2 steps involving minimum protecting group manipulations. We can cleave the diphenylphosphate group for further synthetic objectives. 
DOI: 10.1039/c3cc47180b


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