Separation of NH and NH 2 Resonances in ‘ H-Detected Heteronuclear Multiple-Quantum Correlation Spectra

Abstract

15N-lH heteronuclear multiple-quantum correlation spectroscopy (HMQC) (I, 2) is a useful technique for facilitating the sequential assignment of proteins with ‘H NMR spectra that are too complex for analysis by conventional homonuclear experiments alone (3,4). The 15N-‘H HMQC experiment is particularly useful for the study of proteins in the molecular… (More)

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