Quantitative LC-ESI-MS analyses of microcystins and nodularin-R in animal tissue--matrix effects and method validation.

@article{Karlsson2005QuantitativeLA,
  title={Quantitative LC-ESI-MS analyses of microcystins and nodularin-R in animal tissue--matrix effects and method validation.},
  author={Krister M Karlsson and Lisa E. M. Spoof and Jussi Meriluoto},
  journal={Environmental toxicology},
  year={2005},
  volume={20 3},
  pages={381-9}
}
The matrix effects and signal response in LC-MS analysis of six microcystins and nodularin-R were studied in mussels and liver samples from the common eider and rainbow trout. The instrumentation used in the study was a triple quadrupole MS with electrospray ionization. The results from the spiked tissue samples showed that both signal suppression and enhancement occurred. The recorded matrix effects were not severe; all studied toxins could be detected with sufficient limit of detection in all… CONTINUE READING

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