Preparation of LiZnPO4·H2O via a novel modified method and its non-isothermal kinetics and thermodynamics of thermal decomposition

@article{Chen2011PreparationOL,
  title={Preparation of LiZnPO4·H2O via a novel modified method and its non-isothermal kinetics and thermodynamics of thermal decomposition},
  author={Zhipeng Chen and Qian Chai and Sen Liao and Yu‐Dan He and Wenwei Wu and B. Li},
  journal={Journal of Thermal Analysis and Calorimetry},
  year={2011},
  volume={108},
  pages={1235-1242}
}
The single phase α-LiZnPO4·H2O was directly synthesized via solid-state reaction at room temperature using LiH2PO4·H2O, ZnSO4·7H2O, and Na2CO3 as raw materials. XRD analysis showed that α-LiZnPO4·H2O was a compound with orthorhombic structure. The thermal process of α-LiZnPO4·H2O experienced two steps, which involved the dehydration of one crystal water molecule at first, and then the crystallization of LiZnPO4. The DTA curve had the one endothermic peak and one exothermic peak, respectively… Expand

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