New double molybdate Na9Fe(MoO4)6: Synthesis, structure, properties

@article{Savina2013NewDM,
  title={New double molybdate Na9Fe(MoO4)6: Synthesis, structure, properties},
  author={A. Savina and S. F. Solodovnikov and O. M. Basovich and Z. A. Solodovnikova and D. Belov and K. Pokholok and I. Gudkova and S. Stefanovich and B. Lazoryak and E. G. Khaikina},
  journal={Journal of Solid State Chemistry},
  year={2013},
  volume={205},
  pages={149-153}
}
A new double molybdate Na9Fe(MoO4)6 was synthesized using solid state reactions and studied with X-ray powder diffraction, second harmonic generation (SHG) technique, differential scanning calorimetry, X-ray fluorescence analysis, Mossbauer and dielectric impedance spectroscopy. Single crystals of Na9Fe(MoO4)6 were obtained and its structure was solved (the space group R3, a¼14.8264(2), c ¼19.2402(3) A, V¼3662.79(9) A 3 , Z ¼6, R ¼0.0132). The structure is related to that of sodium ion 
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A new Tl4.86Fe0.82Hf1.18(MoO4)6 ternary molybdate: crystal structure and properties.
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