Multiresidue pesticide analysis in fresh produce by capillary gas chromatography-mass spectrometry/selective ion monitoring (GC-MS/SIM) and -tandem mass spectrometry (GC-MS/MS).

@article{Wong2010MultiresiduePA,
  title={Multiresidue pesticide analysis in fresh produce by capillary gas chromatography-mass spectrometry/selective ion monitoring (GC-MS/SIM) and -tandem mass spectrometry (GC-MS/MS).},
  author={Jon W Wong and Kai Zhang and K. VIJAY KUMAR M. Tech and Douglas G Hayward and Carolyn M Makovi and Alexander J. Krynitsky and Frank J. Schenck and Kaushik Banerjee and Soma Dasgupta and Don Keith Brown},
  journal={Journal of agricultural and food chemistry},
  year={2010},
  volume={58 10},
  pages={5868-83}
}
A multiresidue method for the analysis of pesticides in fresh produce has been developed using salt-out acetonitrile extraction, solid-phase dispersive cleanup with octadecyl-bonded silica (C(18)), and graphitized carbon black/primary-secondary amine (GCB/PSA) sorbents and toluene, followed by capillary gas chromatography-mass spectrometry in selected ion monitoring mode (GC-MS/SIM) or -tandem mass spectrometry (GC-MS/MS). Quantitation was determined from calibration curves using matrix-matched… CONTINUE READING

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