Minimizing the t1-noise when using an indirect 1H high-resolution detection of unlabeled samples.

Abstract

The most utilized through-space correlation 1H-{X} methods with proton indirect detection use two consecutive transfers, 1H → X and then X → 1H, with the evolution time t1 in the middle. When the X isotope is not 100% naturally abundant (NA), only the signal of the protons close to these isotopes is modulated by the 1H-X dipolar interactions. This signal is… (More)
DOI: 10.1016/j.ssnmr.2017.06.008

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