Liquid chromatography-atmospheric pressure photoionization-mass spectrometry analysis of triacylglycerol lipids--effects of mobile phases on sensitivity.

@article{Cai2007LiquidCP,
  title={Liquid chromatography-atmospheric pressure photoionization-mass spectrometry analysis of triacylglycerol lipids--effects of mobile phases on sensitivity.},
  author={Sheng-Suan Cai and Luke Chandler Short and Jack A Syage and Michael A Potvin and Jonathan M. Curtis},
  journal={Journal of chromatography. A},
  year={2007},
  volume={1173 1-2},
  pages={88-97}
}
In this work, we evaluate the performance of liquid chromatography-atmospheric pressure photoionization-mass spectrometry (LC-APPI-MS) for non-aqueous reversed phase analysis of six triacylglycerol model compounds using six binary mobile phases including MeOH/iPrOH, MeOH/CHCl(3), MeOH/CH(2)Cl(2), CH(3)CN/iPrOH, CH(3)CN/CHCl(3), and CH(3)CN/CH(2)Cl(2). All mobile phases give comparably good separation performance on a Gemini C(18) column with carefully adjusted gradient elution programs. APPI… CONTINUE READING

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