Liquid chromatographic method with immunoaffinity column cleanup for determination of ochratoxin A in barley: collaborative study.

@article{Entwisle2000LiquidCM,
  title={Liquid chromatographic method with immunoaffinity column cleanup for determination of ochratoxin A in barley: collaborative study.},
  author={A C Entwisle and Adrian C. Williams and Paul J Mann and Paul Slack and J{\"o}el Gilbert},
  journal={Journal of AOAC International},
  year={2000},
  volume={83 6},
  pages={1377-83}
}
A collaborative study was conducted to evaluate a liquid chromatographic (LC) method with immunoaffinity column cleanup for determination of ochratoxin A. The method was tested at 3 concentration levels of ochratoxin A in barley, which represent possible future European regulatory limits. The test portion was extracted with acetonitrile-water by blending at high speed. The extract was filtered, diluted with phosphate-buffered saline (PBS), and applied to an ochratoxin A immunoaffinity column… CONTINUE READING

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Assessment of Dietary Intake of Ochratoxin A by the Population of EU Member States

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