Isolation of dinophysistoxin-2 and the high-performance liquid chromatographic analysis of diarrhetic shellfish toxins using derivatisation with 1-bromoacetylpyrene.

@article{Kelly1996IsolationOD,
  title={Isolation of dinophysistoxin-2 and the high-performance liquid chromatographic analysis of diarrhetic shellfish toxins using derivatisation with 1-bromoacetylpyrene.},
  author={S. S. Kelly and Andrea G. Bishop and E. P. Carmody and K. James},
  journal={Journal of chromatography. A},
  year={1996},
  volume={749 1-2},
  pages={
          33-40
        }
}
  • S. S. Kelly, Andrea G. Bishop, +1 author K. James
  • Published 1996
  • Chemistry, Medicine
  • Journal of chromatography. A
  • The rare diarrhetic shellfish toxin, dinophysistoxin-2 (DTX-2), was isolated from the digestive glands of mussels (Mytilus edulis). This was achieved by chromatography on silica and Sephadex LH-20 followed by reversed-phase solid phase extraction and semi-preparative high-performance liquid chromatography (HPLC) with an Ultremex C18 column. Using 1-bromoacetylpyrene (BAP), as a precolumn derivatisation reagent, the diarrhetic shellfish toxins, okadaic acid (OA), dinophysistoxin-1 (DTX-1) and… CONTINUE READING
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