Identification of a new diarrhoetic toxin in shellfish using liquid chromatography with fluorimetric and mass spectrometric detection.

@article{James1997IdentificationOA,
  title={Identification of a new diarrhoetic toxin in shellfish using liquid chromatography with fluorimetric and mass spectrometric detection.},
  author={K. James and E. P. Carmody and M. Gillman and S. S. Kelly and R. Draisci and L. Lucentini and L. Giannetti},
  journal={Toxicon : official journal of the International Society on Toxinology},
  year={1997},
  volume={35 6},
  pages={
          973-8
        }
}
  • K. James, E. P. Carmody, +4 authors L. Giannetti
  • Published 1997
  • Chemistry, Medicine
  • Toxicon : official journal of the International Society on Toxinology
  • A new toxin, dinophysistoxin-2B (DTX-2B) was isolated from Irish mussels using silica chromatography, gel permeation, octadecylsilane solid-phase extraction and repeated preparative high-performance liquid chromatography (HPLC). Dinophysistoxin-2 (DTX-2) was also isolated from shellfish using the same procedures. The separation of these toxins in chromatographic fractions was monitored using fluorimetric HPLC following derivatization with 9-anthrylmethyldiazomethane or 1-bromoacetylpyrene. Flow… CONTINUE READING
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