HNCO-based measurement of one-bond amide 15N-1H couplings with optimized precision.

Abstract

A pair of 3D HNCO-based experiments have been developed with the aim of optimizing the precision of measurement of (1)J(NH) couplings. Both pulse sequences record (1)J(NH) coupling evolution during the entire constant time interval that (15)N magnetization is dephasing or rephasing with respect to the directly bonded (13)C' nucleus, with (15)N(13)C… (More)
DOI: 10.1007/s10858-009-9391-2

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Cite this paper

@article{Arbogast2010HNCObasedMO, title={HNCO-based measurement of one-bond amide 15N-1H couplings with optimized precision.}, author={Luke W Arbogast and Ananya K Majumdar and Joel R. Tolman}, journal={Journal of biomolecular NMR}, year={2010}, volume={46 2}, pages={175-89} }