Growth of Sb(2)E(3) (E = S, Se) polygonal tubular crystals via a novel solvent-relief-self-seeding process.

@article{Zheng2002GrowthOS,
  title={Growth of Sb(2)E(3) (E = S, Se) polygonal tubular crystals via a novel solvent-relief-self-seeding process.},
  author={Xiuwen Zheng and Yi Xie and Liying Zhu and Xuchuan Jiang and Yunbo Jia and Wenhai Song and Yuping Sun},
  journal={Inorganic chemistry},
  year={2002},
  volume={41 3},
  pages={455-61}
}
A novel solvent-relief-self-seeding (SRSS) process was applied to grow bulk polygonal tubular single crystals of Sb(2)E(3) (E = S, Se), using SbCl(3) and chalcogen elements E (E = S, Se) as the raw materials at 180 degrees C for 7 days in ethanol solution. The products were characterized by various techniques, including X-ray powder diffraction (XRD… CONTINUE READING