Functionalization of SBA-15 by an Acid-Catalyzed Approach. A Surface Characterization Study
@article{Garca2007FunctionalizationOS, title={Functionalization of SBA-15 by an Acid-Catalyzed Approach. A Surface Characterization Study}, author={N. Garc{\'i}a and E. Benito and J. Guzm{\'a}n and P. Tiemblo and V. Morales and R. Garc{\'i}a}, journal={Microporous and Mesoporous Materials}, year={2007}, volume={106}, pages={129-139} }
The functionalization of a mesoporous ordered silica, SBA-15, by a grafting strategy has been successfully achieved. The derivatized SBA-15 products with trimethylmethoxy silane, vinyltrimethoxy silane and octyltrimethoxy silane have been characterized by BET analysis, DRX analysis, thermogravimetric analysis and NMR techniques. The use of p-toluenesulfonic acid as catalyst and the azeotropic distillation of the alcohol generated in the hydrolysis and condensation of the silanes allowed the… Expand
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References
SHOWING 1-10 OF 67 REFERENCES
Functionalization of SBA-15 with APTES and Characterization of Functionalized Materials
- Chemistry
- 2003
- 574
Direct syntheses of ordered SBA-15 mesoporous materials containing arenesulfonic acid groups
- Chemistry
- 2002
- 265
Surface Characterization and Functionalization of MCM-41 Silicas via Silazane Silylation
- Chemistry
- 2000
- 166
Enantioselective styrene epoxidation using the Jacobsen catalyst immobilized on functionalized SBA-15
- Chemistry
- 2005
- 7
Direct synthesis and post-oxidation of SBA-15 and MCM-41 functionalized with butenyl groups
- Chemistry
- 2005
- 3
Active sites on SBA-15 in the Beckmann rearrangement of cyclohexanone oxime to ε-caprolactam
- Chemistry
- 2006
- 42
Direct method for surface silyl functionalization of mesoporous silica.
- Chemistry, Medicine
- Langmuir : the ACS journal of surfaces and colloids
- 2004
- 84
- PDF
Pyridine-15N: A mobile NMR sensor for surface acidity and surface defects of mesoporous silica
- Chemistry
- 2003
- 186
- PDF