Factorial design for Fe, Cu, Zn, Se and Pb preconcentration optimization with APDC and analysis with a portable X-ray fluorescence system.

Abstract

Preconcentration of heavy metals in water with ammonium pyrrolydine dithiocarbamate (APDC) is a common practice in analytical chemistry. A literature review on this topic showed that several authors use this precipitation agent, but in different preconcentration conditions, conducting to divergent results. The objective of this work is to use factorial… (More)
DOI: 10.1016/j.talanta.2007.03.004

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