Electrolytic partial fluorination of organic compounds. 42.(1) marked solvent effects on regioselective anodic monofluorination of 4-oxo-2-pyrimidyl sulfides.


Regioselective anodic monofluorination of 4-oxo-2-pyrimidyl sulfides was investigated under various electrolytic conditions. Anodic fluorination was successfully carried out using Et(4)NF.4HF in dimethoxyethane (DME) to provide the corresponding alpha-fluorinated products in good yields. In contrast, acetonitrile (MeCN) was not suitable for the anodic… (More)


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