Dose formulation and analysis of diapocynin.

  title={Dose formulation and analysis of diapocynin.},
  author={Ron Luchtefeld and Rensheng Luo and Keith J. Stine and Mikaela L Alt and Patricia A Chernovitz and Robert Elliot Smith},
  journal={Journal of agricultural and food chemistry},
  volume={56 2},
Procedures based on high-performance liquid chromatography (HPLC) with ultraviolet (UV) detection and liquid chromatography-mass spectrometry (LC-MS) are described for analyzing diapocynin. Diapocynin was synthesized by oxidative coupling of two apocynin monomers, through the in situ generation of sulfate radicals. It was purified by washing 3 times each… CONTINUE READING