Dioxidouranium isothiosemicarbazone coordination compounds: synthesis, characterization, crystal structure, and thermal behavior

@inproceedings{Takjoo2018DioxidouraniumIC,
  title={Dioxidouranium isothiosemicarbazone coordination compounds: synthesis, characterization, crystal structure, and thermal behavior},
  author={Reza Takjoo and Joel T. Mague},
  year={2018}
}
AbstractFive uranium complexes with UO2L′(solv) formula (L′: prepared by condensation reaction between 2-hydroxyacetophenon S-pentyl isothiosemicarbazone (H2L) and 5-bromosalicylaldehyde (Sal); solv: ethanol (1), 2-propanol (2), 2-butanol (3), ethylene glycol (4), 1,2-propanediol (5)) were synthesized through template reactions between H2L, Sal, and UO2(CH3COO)2∙2H2O for 1 and recrystallization of 1 in appropriate solvents for the other complexes. The compounds are characterized by melting… CONTINUE READING