Development of a solid-phase microextraction gas chromatography with microelectron-capture detection method for a multiresidue analysis of pesticides in bovine milk.

@article{Fernndezlvarez2008DevelopmentOA,
  title={Development of a solid-phase microextraction gas chromatography with microelectron-capture detection method for a multiresidue analysis of pesticides in bovine milk.},
  author={Mar{\'i}a Fern{\'a}ndez-{\'A}lvarez and Maria Llompart and J Pablo Lamas and Marta Lores and Carmen Garc{\'i}a-Jares and Rafael Cela and Thierry Dagnac},
  journal={Analytica chimica acta},
  year={2008},
  volume={617 1-2},
  pages={37-50}
}
A simple and rapid method based on solid-phase microextraction (SPME) technique followed by gas chromatography with microelectron-capture detection (GC-microECD) was developed for the simultaneous determination of more than 30 pesticides (pyrethroids and organochlorinated among others) in milk. To our knowledge, this is the first application of SPME for the determination of pyrethroid pesticides in milk. Negative matrix effects due to the complexity and lipophility of the studied matrix were… CONTINUE READING
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