Development, optimization and validation of a multimethod for the determination of 36 mycotoxins in wines by liquid chromatography-tandem mass spectrometry.

@article{Pizzutti2014DevelopmentOA,
  title={Development, optimization and validation of a multimethod for the determination of 36 mycotoxins in wines by liquid chromatography-tandem mass spectrometry.},
  author={Ionara Regina Pizzutti and Andr{\'e} de Kok and J. H. M. Scholten and La{\'i}s W Righi and Carmem Dickow Cardoso and Graciele Necchi Rohers and Rosselei C da Silva},
  journal={Talanta},
  year={2014},
  volume={129},
  pages={352-63}
}
A fast and efficient multimethod for the determination of 36 mycotoxins in wine, using ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS), was developed, optimized, validated and implemented in routine analysis. A simplified, quick extraction was performed with acetonitrile, derived from the QuEChERS (quick, easy, cheap, effective, rugged and safe) approach, which was traditionally developed for pesticides analysis. This study aimed at a single extraction and… CONTINUE READING

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