Determination of tilmicosin residues in chicken, cattle, swine, and sheep tissues by liquid chromatography.

@article{StobbaWiley2000DeterminationOT,
  title={Determination of tilmicosin residues in chicken, cattle, swine, and sheep tissues by liquid chromatography.},
  author={C M Stobba-Wiley and J. P. Chang and Dimity Elsbury and John W Moran and James M Turner and Robin S Readnour},
  journal={Journal of AOAC International},
  year={2000},
  volume={83 4},
  pages={837-46}
}
A method was developed and validated for determination and quantitation of tilmicosin residues in swine, cattle, and sheep edible tissues, as well as chicken fat, skin, and muscle over a concentration range of 0.025 microg/g-20 microg/g. For chicken kidney and liver, the method was validated over a range of 0.060 microg/g-20 microg/g. The tissue sample was extracted with methanol and a C18 cartridge was used for solid-phase extraction cleanup. A reversed-phase gradient liquid chromatographic… CONTINUE READING

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