Determination of spiroxamine residues in grapes, must, and wine by gas chromatography/ion trap-mass spectrometry.

N. Tsiropoulos; K. Liapis; D. T. Likas; G. Miliadis

DOI:10.1093/JAOAC/88.6.1834

Corpus ID: 46458362

Determination of spiroxamine residues in grapes, must, and wine by gas chromatography/ion trap-mass spectrometry.

@article{Tsiropoulos2005DeterminationOS,
  title={Determination of spiroxamine residues in grapes, must, and wine by gas chromatography/ion trap-mass spectrometry.},
  author={N. Tsiropoulos and K. Liapis and D. T. Likas and G. Miliadis},
  journal={Journal of AOAC International},
  year={2005},
  volume={88 6},
  pages={
          1834-9
        }
}

N. Tsiropoulos, K. Liapis, +1 author G. Miliadis

Published 2005

Chemistry, Medicine

Journal of AOAC International

Analytical methodology was developed and validated for the determination of spiroxamine residues in grapes, must, and wine by gas chromatography/ion trap-mass spectrometry (GC/IT-MS). Two extraction procedures were used: the first involved grapes, must, and wine extraction with alkaline cyclohexane-dichloromethane (9 + 1, v/v) solution, and the second grape extraction with acetone, dichloromethane, and petroleum ether. In both procedures, the extract was centrifuged, evaporated to dryness, and… CONTINUE READING

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