Determination of hexabromocyclododecane diastereoisomers in air and soil by liquid chromatography-electrospray tandem mass spectrometry.

@article{Yu2008DeterminationOH,
  title={Determination of hexabromocyclododecane diastereoisomers in air and soil by liquid chromatography-electrospray tandem mass spectrometry.},
  author={Zhiqiang Yu and Ping'an Peng and Guoying Sheng and Jiamo Fu},
  journal={Journal of chromatography. A},
  year={2008},
  volume={1190 1-2},
  pages={74-9}
}
Hexabromocyclododecanes (HBCDs), used as additive brominated flame retardants, are of high concern due to their widespread use and increasing levels in various environmental systems. High-performance liquid chromatography coupled with electrospray ionization tandem mass spectrometry (LC-MS/MS) was developed for the determination of HBCD diastereoisomers. A detailed study was carried out to optimize the composition of the mobile phase involving methanol/acetonitrile/water, and the values of MS… CONTINUE READING

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