Determination of endocrine-disrupting phenols in water samples by a new manual shaking-enhanced, ultrasound-assisted emulsification microextraction method.

@article{Shu2012DeterminationOE,
  title={Determination of endocrine-disrupting phenols in water samples by a new manual shaking-enhanced, ultrasound-assisted emulsification microextraction method.},
  author={Ming-Wei Shu and Mei-I Leong and M S Fuh and Shang-Da Huang},
  journal={The Analyst},
  year={2012},
  volume={137 9},
  pages={2143-50}
}
Manual shaking-enhanced, ultrasound-assisted emulsification microextraction (MS-USAEME) combined with ultraperformance liquid chromatography (UPLC) with UV detection has been developed for the determination of five endocrine-disrupting phenols (EDPs) in seawater samples and detergent samples: 4-tert-butylphenol (4-t-BP), 4-cumylphenol (4-CP), 4-tert-octylphenol (4-t-OP), 2,4-di-tert-butylphenol (2,4-di-t-BP) and 4-nonylphenol (4-NP). Optimum conditions were found to be: 25 μL 1-bromohexadecane… CONTINUE READING
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