Determination of dimethyl fumarate (DMFu) in silica gel pouches using gas chromatography coupled ion trap mass spectrometry.

@article{Stefanelli2011DeterminationOD,
  title={Determination of dimethyl fumarate (DMFu) in silica gel pouches using gas chromatography coupled ion trap mass spectrometry.},
  author={Patrizia Stefanelli and Danilo Attard Barbini and Silvana Girolimetti and Angela Santilio and Roberto Dommarco},
  journal={Journal of environmental science and health. Part. B, Pesticides, food contaminants, and agricultural wastes},
  year={2011},
  volume={46 4},
  pages={
          341-9
        }
}
  • Patrizia Stefanelli, Danilo Attard Barbini, +2 authors Roberto Dommarco
  • Published in
    Journal of environmental…
    2011
  • Medicine, Chemistry
  • A simple method for the determination of dimethyl fumarate (DMFu) in silica gel pouches has been developed. The gas chromatographic behaviour of DMFu was investigated; the instrumental method, based on EI mass spectrometry coupled with an Ion Trap Detector operating whether in full scan mode or in MS/MS mode was also investigated. Several factors have been evaluated and optimized during the development process: solvent and temperature of extraction, type of stationary phase in capillary column… CONTINUE READING

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