Determination of cymiazole residues in honey by liquid chromatography.

  title={Determination of cymiazole residues in honey by liquid chromatography.},
  author={Paolo Cabras and Marinella Melis and L Spanedda},
  journal={Journal of AOAC International},
  volume={76 1},
A liquid chromatographic method is described for the determination of cymiazole residues in honey. This acaricide is determined on a reversed-phase (C18) column, with a CH3CN-0.001N HCl-NaCl mixture (950 mL + 50 mL + 0.3 g/L) as the mobile phase, and UV detection at 265 nm. Cymiazole is extracted with n-hexane from aqueous alkalinized (pH 9) honey solutions. No further cleanup of the honey extract was required before chromatographic analysis. Recoveries on control samples fortified with 0.01, 0… CONTINUE READING

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