Determination of biogenic amines in wines by pre-column derivatization and high-performance liquid chromatography coupled to mass spectrometry.

@article{GarcaVillar2009DeterminationOB,
  title={Determination of biogenic amines in wines by pre-column derivatization and high-performance liquid chromatography coupled to mass spectrometry.},
  author={Natividad Garc{\'i}a-Villar and Santiago Hern{\'a}ndez-Cassou and Javier Saurina},
  journal={Journal of chromatography. A},
  year={2009},
  volume={1216 36},
  pages={
          6387-93
        }
}
A new HPLC method for determining biogenic amines in wines is developed. This method is based on pre-column amine derivatization, further separation of derivatives and on-line hyphenation of HPLC to atmospheric pressure chemical ionization mass spectrometry (APCI-MS). Biogenic amines have been derivatized with 1,2-naphthoquinone-4-sulfonate at 65 degrees C and pH 9.2 for 5 min. The separation of derivatives has been accomplished in a C(18) analytical column using an elution gradient based on… CONTINUE READING
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