Determination of aliphatic and alicyclic amines in water by gas and liquid chromatography after derivatization by chloroformates.

@article{Pietsch1996DeterminationOA,
  title={Determination of aliphatic and alicyclic amines in water by gas and liquid chromatography after derivatization by chloroformates.},
  author={J{\"o}rg Pietsch and S. Hampel and Wido Schmidt and H J Brauch and Eckhard Worch},
  journal={Analytical and bioanalytical chemistry},
  year={1996},
  volume={355 2},
  pages={164-73}
}
Two new methods were developed for the analysis of aliphatic (n-propylamine, pentylamine, hexylamine, heptylamine, octylamine) and alicyclic (pyrrolidine, morpholine, piperidine, piperazine) amines in water samples after derivatization and liquid-liquid-extraction. The carbamate-derivatives formed were determined by GC/MS (trichloroethyl carbamates) as well as by HPLC/fluorescence detection (9-fluorenylmethyl carbamates) in a concentration range between 0.05 and 1.0 microg/l suitable for… CONTINUE READING

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