Corpus ID: 101751445

Determination of 2,3-cyclopentenopyridine by gas chromatography

  title={Determination of 2,3-cyclopentenopyridine by gas chromatography},
  author={Dong Jian-fang},
  journal={Hebei Journal of Industrial Science and Technology},
  • Dong Jian-fang
  • Published 2008
  • Chemistry
  • Hebei Journal of Industrial Science and Technology
By optimizing separation conditions of gas chromatography(GC),a method has been developed for the determination of 2,3-cyclopentenopyridine by using GC.The GC conditions are as follows:capillary column,SE-30,25 m×0.22 mm×0.25 μm;carrier gas(N_2) velocity is 1.0 mL/min;oven temperature is 130 ℃;inlet temperature is 200 ℃;split ratio is 100∶1.The samples of 2,3-cyclopentenopyridine synthesized are tested.The linear equation is A=440.84 c+33 088,r=0.999 3.The linear range is 2~500 mg/L.The… Expand
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